| Author | dc.contributor.author | Núñez Vergara, Luis | es_CL |
| Author | dc.contributor.author | Navarrete Encina, Patricio | es_CL |
| Author | dc.contributor.author | Salas, S. | es_CL |
| Author | dc.contributor.author | Conde, B. | es_CL |
| Author | dc.contributor.author | Carbajo, J. | es_CL |
| Author | dc.contributor.author | Squella Serrano, Juan | es_CL |
| Author | dc.contributor.author | Camargo Grandón, Rodrigo | |
| Admission date | dc.date.accessioned | 2008-08-28T15:38:44Z | |
| Available date | dc.date.available | 2008-08-28T15:38:44Z | |
| Publication date | dc.date.issued | 2007-05-09 | |
| Cita de ítem | dc.identifier.citation | JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS 44(1):236-242 | en |
| Identifier | dc.identifier.issn | 0731-7085 | |
| Identifier | dc.identifier.uri | https://repositorio.uchile.cl/handle/2250/120473 | |
| Abstract | dc.description.abstract | El mass spectra of products of the dihydropyridine Hantzsch synthesis using hydroxy and methoxy aldehydes as starting materials are reported. The reaction products (C-4 hydroxy- and methoxyphenyl-1,4-dihydropyridines and chromeno[3,4,c]-pyridines) were derivatized with N-methyl-N-(trimethylsilyl)-trifluoracetamide to be analyzed by gas chromatographic techniques. Fragmentation pathways for 1,4-dihydropyridines and chromeno-pyridines are proposed. The study provides (mainly through MS-MS technique) useful data for the confirmation of the structure of the compounds and also is a valuable tool for further analytical purposes to follow both photostability and reactivity studies with free radicals for these types of compounds. | en |
| Lenguage | dc.language.iso | en | en |
| Publisher | dc.publisher | PERGAMON-ELSEVIER SCIENCE | en |
| Keywords | dc.subject | GC-MS | en |
| Título | dc.title | Analyses by GC-MS and GC-MS-MS of the hantzsch synthesis products using hydroxy- and methoxy-aromatic aldehydes | en |
| Document type | dc.type | Artículo de revista | |
