| Author | dc.contributor.author | Galdámez Silva, Antonio | |
| Author | dc.contributor.author | Castro Castillo, Vicente | es_CL |
| Author | dc.contributor.author | Cassels Niven, Bruce | es_CL |
| Admission date | dc.date.accessioned | 2012-06-04T19:42:35Z | |
| Available date | dc.date.available | 2012-06-04T19:42:35Z | |
| Publication date | dc.date.issued | 2009-07-03 | |
| Cita de ítem | dc.identifier.citation | J. Chil. Chem. Soc., Vol. 54, Nº 3, 2009. | es_CL |
| Identifier | dc.identifier.issn | 0717-9707 | |
| Identifier | dc.identifier.uri | https://repositorio.uchile.cl/handle/2250/119446 | |
| Abstract | dc.description.abstract | The title compound was prepared by cyclization of 2-(3,4-methylenedioxyphenyl)ethyl-3-hydroxyisoindolin-1-one in concentrated hydrochloric acid. The compound crystallizes in the orthorhombic space group Pca21 (No. 29) with a = 27.034(5) Å, b = 4.5093(9) Å, c = 10.667(2)Å, V = 1300.4(4) Å3 and Z = 4. The crystal consists of a single enantiomer. The molecule consists of two essentially flat moieties forming an dihedral angle of 116.3(2)º. The crystal structure has intermolecular C-H⋅⋅⋅O interactions resulting in chains that run along the crystallographic c-axis. | es_CL |
| Patrocinador | dc.description.sponsorship | V. C.-C. is the recipient of a MeceSup (UMCE-0204) fellowship. M. T. Garland and A. Ibáñez are thanked for the X-ray measurements and FONDAP Grant Nº 11980002 for the purchase of the Bruker SMART CCD single crystal diffractometer. This work was supported in part by CONICYT grant AT-23070040 and ICM grant P05-001-F. | es_CL |
| Lenguage | dc.language.iso | en | es_CL |
| Publisher | dc.publisher | Sociedad Chilena de Química | es_CL |
| Keywords | dc.subject | crystal structure | es_CL |
| Título | dc.title | CRYSTAL STRUCTURE OF 5,6,8,12b-TETRAHYDRODIOXOLO[4,5-g]ISOINDOLO[1,2-a]ISOQUINOLIN-8-ONE (C17H13NO3) | es_CL |
| Document type | dc.type | Artículo de revista | |
