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Spectral Assignments and Reference Data Complete 1H and 13C NMR spectral assignment of hydrogenated oxoisoaporphine derivatives

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2003-03-10
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Sobarzo Sánchez, Eduardo
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Spectral Assignments and Reference Data Complete 1H and 13C NMR spectral assignment of hydrogenated oxoisoaporphine derivatives
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Author
  • Sobarzo Sánchez, Eduardo;
  • Cassels Niven, Bruce;
  • Castedo, Luis;
Abstract
2,3,8,9,10,11-Hexahydro-7H-dibenzo[de,h]quinolin-7- one, 5-methoxy-2,3,8,9,10,11-hexahydro-7H-dibenzo[de,h] quinolin-7-one, 5-methoxy-6-hydroxy-1,2,3,7a,8,9,10,11, 11a,11b-decahydro-7H-dibenzo[de,h]quinolin-7-one, 5- methoxy-5,6,8,9,10,11-hexahydro-4H-dibenzo[de,h]quinolin- 7-ol, 5,6,8,9,10,11-hexahydro-4H-dibenzo[de,h]quinolin- 7-ol and 5,6-dihydro-4H-dibenzo[de,h]quinolin-7-ol were prepared by catalytic hydrogenation of oxoisoaporphines or their 2,3-dihydro derivatives over PtO2 in acetic acid under mild conditions. Their structures were confirmed and 1H and 13C NMR spectra were completely assigned using a combination of one- and two-dimensional NMR techniques. Copyright  2003 John Wiley & Sons, Ltd.
Patrocinador
E.S.-S. thanks Fundaci´on Andes for a scholarship. This work was supported in part by FONDECYT Grant No. 2010056.
Identifier
URI: https://repositorio.uchile.cl/handle/2250/119483
ISSN: 1097-458X
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MAGNETIC RESONANCE IN CHEMISTRY, Vol. 41, p. 545–548, 2003.
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